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By J R Hanson; James Ralph Hanson; Royal Society of Chemistry (Great Britain); et al
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Additional info for A review of the literature published between September 1975 & August 1976
Muscio, and R. J. Goodfellow, Biochemistry, 1974, 13, 1530 and J. Org. , 1975, 40, 139, were omitted from last year's Report. 216 Racemic methyl santolinate (82) was synthesized (along with the C-3 epimer; ratio 8 : 1) via Claisen rearrangement, according to Scheme 2 (cf. Vol. 6 , p. 217 OSiMe,Bu' lvii-ix H (82) Reagents: i, NaCH(CO,Et)PO(OEt),; ii, LiAIH,; iii, (EtCO)20-py; iv, lithium isopropylcyclohexylamideTHF, -78 "C; v, HMPA-Bu'SiMezC1-THF; vi, NaCI, 0 "C; vii, 65 "C; viii, AcOH-H20; ix, CH2N2.
S. 5; X = OH) and Table 1 refers to CO instead of C 0 2 . R. Antkowiak and W. Z . Antkowiak, Bull. A c a d . polon. , Sir. Sci. , 1976, 24. 291; the corresponding ketone may have been formed by Bardyshev as ketone X, I. I . , V. Kosnikova, A. L. Pertsovskii, and L. M. Krezo, Doklady A k a d . , 1969,186, 1325 (Chem. , 1969,71, 102 022). R. Antkowiak and W. Z. Antkowiak, Bull. A c a d . polon. , Sir. Sci. , 1976, 24, 299; cf. Vol. 2, p, 43 for the formation of (198) via acetolysis of fenchyl toluene-p-sulphonate.
69 049/1975 (Chem. A h . , 1975,83, 193 551). 290 29l Monoterpenoids 31 Last year's Report of (+)-limonene hydroboration (Vol. 6, p. 30) did not refer to the earlier Report (Vol. 3, p. 35) which, in the case of Brown's work, is a repetition of earlier Bacdyshev reports the salicylic acid-catalysed rearrangement of isoterpinolene to various p-methadienes (cf. Vol. 3, p. 71, ref. 304 Pyrolysis of limonene diacetate yields perillyl acetate as the major The full paper on the oxidation of cis- and trans-p-menth-2-ene with t-duty1 perbenzoate-cupric octanoate has appeared (Vol.
A review of the literature published between September 1975 & August 1976 by J R Hanson; James Ralph Hanson; Royal Society of Chemistry (Great Britain); et al